Technology Transfer Network
Emission Measurement Center Spectral Database
Table 6-5. Compounds Meeting Method 301
Criteria in Concentrated Samples
Benzene-015
SPIKED DEV. UNSPIKED DEV.
19.95 1.94
22.03 2.08 1.61 -0.33
16.88 0.13
20.74 3.86 0.48 0.35
19.90 5.93 1.04 0.01
RSD= 8.99 RSD= 18.86
Bias= -1.14 Exp Conc= 20.00
t= 0.63 CF= 1.06
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Chlorobenzene-037
SPIKED DEV. UNSPIKED DEV.
25.84 4.38
29.20 3.36 2.75 -1.62
25.61 1.55
26.40 0.78 2.85 1.30
32.95 3.58
30.32 -2.63 5.54 1.96
28.39 1.51 3.44 1.64
RSD= 6.24 RSD= 33.89
Bias= 4.95 Exp Conc= 20.00
t= 2.33 CF= 0.80
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Ethylene Dibromide-080
SPIKED DEV. UNSPIKED DEV.
21.25 1.80
25.87 4.62 1.67 -0.13
25.75 1.81
25.17 -0.58 3.54 1.73
24.51 4.04 2.20 1.60
RSD= 7.76 RSD= 32.11
Bias= 2.30 Exp Conc= 20.00
t= 1.14 CF= 0.90
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n-Hexane-095
SPIKED DEV. UNSPIKED DEV.
13.88 2.32
23.69 9.81 2.42 0.10
17.51 0.34
15.64 -1.87 0.00 -0.34
17.68 7.95 1.27 -0.24
RSD= 28.26 RSD= 13.92
Bias= -3.59 Exp Conc= 20.00
t= 0.72 CF= 1.22
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Methyl Ethyl Ketone-109
SPIKED DEV. UNSPIKED DEV.
20.30 -2.99
11.94 -8.36 -3.39 -0.39
26.15 -0.91
24.97 -1.18 -1.51 -0.60
27.27 -2.22
23.02 -4.25 -0.88 1.33
22.27 -13.79 -1.98 0.34
RSD= 17.32 RSD= -31.16
Bias= 4.26 Exp Conc= 20.00
t= 1.09 CF= 0.82
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2-Nitropropane-124
SPIKED DEV. UNSPIKED DEV.
21.82 -1.76
22.86 1.04 -1.86 -0.10
20.95 -1.61
21.05 0.10 -0.55 1.06
21.67 1.14 -0.44 0.96
RSD= 2.42 RSD= -37.08
Bias= 3.11 Exp Conc= 20.00
t= 4.16 CF= 0.87
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Tetrachloroethylene-151
SPIKED DEV. UNSPIKED DEV.
20.45 1.90
25.18 4.73 2.16 0.26
13.25 0.39
23.11 9.86 1.74 1.35
20.50 14.59 1.55 1.61
RSD= 26.67 RSD= 44.51
Bias= -1.05 Exp Conc= 20.00
t= 0.19 CF= 1.06
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Toluene-153
SPIKED DEV. UNSPIKED DEV.
28.48 -1.11
22.61 -5.87 -0.66 0.45
22.43 -0.33
22.33 -0.10 -0.29 0.04
23.78 -0.42
22.63 -1.15 -0.12 0.30
23.71 -7.13 -0.49 0.79
RSD= 10.31 RSD= -45.59
Bias= 4.20 Exp Conc= 20.00
t= 1.71 CF= 0.83
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Trichloroethylene-160
SPIKED DEV. UNSPIKED DEV.
27.88 9.10
27.37 -0.51 5.27 -3.83
22.65 1.89
24.63 1.98 4.81 2.92
25.63 1.47 5.27 -0.92
RSD= 3.26 RSD= 37.35
Bias= 0.37 Exp Conc= 20.00
t= 0.17 CF= 0.98
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m-Xylene-172
SPIKED DEV. UNSPIKED DEV.
25.26 0.24
28.15 2.89 0.39 0.15
24.99 0.13
24.61 -0.38 0.22 0.10
27.02 0.42
25.99 -1.04 0.75 0.34
26.00 1.47 0.36 0.58
RSD= 4.85 RSD= 43.31
Bias= 5.65 Exp Conc= 20.00
t= 4.44 CF= 0.78
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p-Xylene-173
SPIKED DEV. UNSPIKED DEV.
11.80 -0.44
16.47 4.67 -0.25 0.19
19.23 -0.24
20.54 1.30 -0.16 0.08
17.01 5.97 -0.28 0.27
RSD= 14.25 RSD= -36.71
Bias= -2.72 Exp Conc= 20.00
t= 1.12 CF= 1.16
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