Parameters With Sampling Methodologies - PAMS

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Last Updated on 11/6/2012 at 8:19:33

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<Parameter Code> <Parameter Desc> <Standard Unit> <Meth Code> <Duration Code> <Duration Desc> <Unit> <Unit Desc> <Collection Desc> <Sample Analysis Disc> <FED MDL> <Summary Scale> <Equivalent Method Desc> <Reference Method ID> <ABS Max Sample Value> <ABS Min Sample Value>

45202 Toluene 078 157 1 1 HOUR 078 Parts per billion Carbon Instrumental Open Path UV OPSIS Model AR 500 14.0 1 None None None -14.0

45202 Toluene 078 168 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PACKED COLUMN GC - ECD/PID 1.4 2 None None None -1.4

45202 Toluene 078 169 7 24 HOUR 078 Parts per billion Carbon TEDLAR BAG PACKED COLUMN GC - ECD/PID 1.4 2 None None None -1.4

45202 Toluene 078 171 7 24 HOUR 078 Parts per billion Carbon 6L Pressurized Canister Precon Saturn GC/MS 0.1 2 None None None -0.1

45202 Toluene 078 172 7 24 HOUR 078 Parts per billion Carbon 6L Pressurized Canister Precon HP GC/MS 0.1 2 None None None -0.1

45202 Toluene 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

45202 Toluene 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

45202 Toluene 078 176 6 12 HOUR 078 Parts per billion Carbon 6L SUBATM SS CANISTER ENTECH PRECONCENTRATOR GC/MS 0.28 2 None None None -0.28

45202 Toluene 078 176 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM SS CANISTER ENTECH PRECONCENTRATOR GC/MS 0.28 2 None None None -0.28

45202 Toluene 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

45202 Toluene 078 210 7 24 HOUR 078 Parts per billion Carbon SS 6L Pressurized Canister Cryogenic Precon GC/MS 0.14 3 None None None -0.14

45202 Toluene 078 211 7 24 HOUR 078 Parts per billion Carbon SS Canister Subambient Pressure Gas Chromatograph Mass Spectro 0.84 2 None None None -0.84

43102 Total NMOC (non-methane organic compound) 078 011 1 1 HOUR 078 Parts per billion Carbon INSTRUMENTAL FLAME IONIZATION 1.0 0 None None 20000.0 -1.0

43102 Total NMOC (non-methane organic compound) 078 012 1 1 HOUR 078 Parts per billion Carbon 6L SS CANISTER-PRESSURIZED CRYOGENIC PRECON FLAME IONI(PDFID) 0.2 1 None None 20000.0 -0.2

43102 Total NMOC (non-methane organic compound) 078 012 3 4 HOUR 078 Parts per billion Carbon 6L SS CANISTER-PRESSURIZED CRYOGENIC PRECON FLAME IONI(PDFID) 0.2 1 None None 20000.0 -0.2

43102 Total NMOC (non-methane organic compound) 078 012 7 24 HOUR 078 Parts per billion Carbon 6L SS CANISTER-PRESSURIZED CRYOGENIC PRECON FLAME IONI(PDFID) 0.2 1 None None 20000.0 -0.2

43102 Total NMOC (non-methane organic compound) 078 012 B 3 HOURS 078 Parts per billion Carbon 6L SS CANISTER-PRESSURIZED CRYOGENIC PRECON FLAME IONI(PDFID) 0.2 1 None None 20000.0 -0.2

43102 Total NMOC (non-methane organic compound) 078 013 1 1 HOUR 078 Parts per billion Carbon INSTRUMENTAL PHOTO IONIZATION 20.0 0 None None 20000.0 -20.0

43102 Total NMOC (non-methane organic compound) 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None 20000.0 -0.01

43102 Total NMOC (non-methane organic compound) 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None 20000.0 -0.01

43102 Total NMOC (non-methane organic compound) 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None 20000.0 -0.01

43102 Total NMOC (non-methane organic compound) 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None 20000.0 -0.01

43102 Total NMOC (non-methane organic compound) 078 124 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID 1.0 1 None None 20000.0 -1.0

43102 Total NMOC (non-methane organic compound) 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 2 None None 20000.0 -0.136

43102 Total NMOC (non-methane organic compound) 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 2 None None 20000.0 -0.136

43102 Total NMOC (non-methane organic compound) 078 125 B 3 HOURS 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 2 None None 20000.0 -0.136

43102 Total NMOC (non-methane organic compound) 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.01 2 None None 20000.0 -0.01

43102 Total NMOC (non-methane organic compound) 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.01 2 None None 20000.0 -0.01

43102 Total NMOC (non-methane organic compound) 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 128 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 129 1 1 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER VARIAN SATURN-2 GC/MS 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 135 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH CRYFOCUS/VARIAN GC/FINN DTMS 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.4 2 None None 20000.0 -0.4

43102 Total NMOC (non-methane organic compound) 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.4 2 None None 20000.0 -0.4

43102 Total NMOC (non-methane organic compound) 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.4 2 None None 20000.0 -0.4

43102 Total NMOC (non-methane organic compound) 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 0.1 4 None None None -0.1

43102 Total NMOC (non-methane organic compound) 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43102 Total NMOC (non-methane organic compound) 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 160 1 1 HOUR 078 Parts per billion Carbon INSTRUMENTAL 8202/8202A:NMOC CAL GAS = METHANE 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 161 1 1 HOUR 078 Parts per billion Carbon INSTRUMENTAL 8202/8202A:NMOC CAL GAS = PROPANE 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 162 1 1 HOUR 078 Parts per billion Carbon INSTRUMENTAL 8202/8202A:NMOC CAL GAS = HEXANE 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 163 B 3 HOURS 078 Parts per billion Carbon 6L-SS-CANISTER-PRESSURIZED CRYOGEN PRECON FID:SUM OF SPECIES 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 164 1 1 HOUR 078 Parts per billion Carbon INSTRUMENTAL TEI 55:NMOC CAL GAS = PROPANE 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 173 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration FID 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 173 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration FID 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 200 1 1 HOUR 078 Parts per billion Carbon INSTRUMENTAL SUM OF PEAKS 0.1 2 None None 30000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 200 3 4 HOUR 078 Parts per billion Carbon INSTRUMENTAL SUM OF PEAKS 0.1 2 None None 30000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 200 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL SUM OF PEAKS 0.1 2 None None 30000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 200 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL SUM OF PEAKS 0.1 2 None None 30000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 300 1 1 HOUR 078 Parts per billion Carbon MISC COLLECTION METHODS WITH SEPARATION OTHER THAN BY GC/FID 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 300 3 4 HOUR 078 Parts per billion Carbon MISC COLLECTION METHODS WITH SEPARATION OTHER THAN BY GC/FID 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 300 7 24 HOUR 078 Parts per billion Carbon MISC COLLECTION METHODS WITH SEPARATION OTHER THAN BY GC/FID 0.1 2 None None 20000.0 -0.1

43102 Total NMOC (non-methane organic compound) 078 300 B 3 HOURS 078 Parts per billion Carbon MISC COLLECTION METHODS WITH SEPARATION OTHER THAN BY GC/FID 0.1 2 None None 20000.0 -0.1

43217 cis-2-Butene 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

43217 cis-2-Butene 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43217 cis-2-Butene 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43217 cis-2-Butene 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43217 cis-2-Butene 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43217 cis-2-Butene 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43217 cis-2-Butene 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43217 cis-2-Butene 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43217 cis-2-Butene 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43217 cis-2-Butene 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43217 cis-2-Butene 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43217 cis-2-Butene 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43217 cis-2-Butene 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43217 cis-2-Butene 078 125 B 3 HOURS 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43217 cis-2-Butene 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43217 cis-2-Butene 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43217 cis-2-Butene 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43217 cis-2-Butene 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43217 cis-2-Butene 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

43217 cis-2-Butene 078 129 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER VARIAN SATURN-2 GC/MS 0.1 1 None None None -0.1

43217 cis-2-Butene 078 135 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH CRYFOCUS/VARIAN GC/FINN DTMS 0.1 1 None None None -0.1

43217 cis-2-Butene 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43217 cis-2-Butene 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43217 cis-2-Butene 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43217 cis-2-Butene 078 141 1 1 HOUR 078 Parts per billion Carbon IR Spectrometer Spectra reference matching with PLS 6.0 1 None None None -6.0

43217 cis-2-Butene 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 0.52384 4 None None None -0.52384

43217 cis-2-Butene 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43217 cis-2-Butene 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43217 cis-2-Butene 078 147 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - SATURN II GC/FID 0.08 2 None None None -0.08

43217 cis-2-Butene 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.08 2 None None None -0.08

43217 cis-2-Butene 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.08 2 None None None -0.08

43217 cis-2-Butene 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.08 2 None None None -0.08

43217 cis-2-Butene 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.08 2 None None None -0.08

43217 cis-2-Butene 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None None -0.1

43217 cis-2-Butene 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None None -0.1

43217 cis-2-Butene 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43217 cis-2-Butene 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43217 cis-2-Butene 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43227 cis-2-Pentene 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43227 cis-2-Pentene 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43227 cis-2-Pentene 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43227 cis-2-Pentene 078 124 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID 1.0 1 None None None -1.0

43227 cis-2-Pentene 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43227 cis-2-Pentene 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43227 cis-2-Pentene 078 125 B 3 HOURS 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43227 cis-2-Pentene 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43227 cis-2-Pentene 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43227 cis-2-Pentene 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

43227 cis-2-Pentene 078 129 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER VARIAN SATURN-2 GC/MS 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 135 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH CRYFOCUS/VARIAN GC/FINN DTMS 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 0.57456 4 None None None -0.57456

43227 cis-2-Pentene 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 147 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - SATURN II GC/FID 0.4 2 None None None -0.4

43227 cis-2-Pentene 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None None -0.1

43227 cis-2-Pentene 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43227 cis-2-Pentene 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43227 cis-2-Pentene 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45218 m-Diethylbenzene 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45218 m-Diethylbenzene 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45218 m-Diethylbenzene 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45218 m-Diethylbenzene 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

45218 m-Diethylbenzene 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

45218 m-Diethylbenzene 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

45218 m-Diethylbenzene 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

45218 m-Diethylbenzene 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

45218 m-Diethylbenzene 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 2.19044 4 None None None -2.19044

45218 m-Diethylbenzene 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 148 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None None -0.1

45218 m-Diethylbenzene 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

45218 m-Diethylbenzene 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

45218 m-Diethylbenzene 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.01 2 None None None -0.01

45212 m-Ethyltoluene 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.01 2 None None None -0.01

45212 m-Ethyltoluene 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45212 m-Ethyltoluene 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45212 m-Ethyltoluene 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45212 m-Ethyltoluene 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45212 m-Ethyltoluene 078 124 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID 1.0 1 None None None -1.0

45212 m-Ethyltoluene 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

45212 m-Ethyltoluene 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

45212 m-Ethyltoluene 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

45212 m-Ethyltoluene 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

45212 m-Ethyltoluene 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

45212 m-Ethyltoluene 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 2.25865 4 None None None -2.25865

45212 m-Ethyltoluene 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 148 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None None -0.1

45212 m-Ethyltoluene 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

45212 m-Ethyltoluene 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

45212 m-Ethyltoluene 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

45109 m/p Xylene 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

45109 m/p Xylene 078 101 6 12 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 2 None None None -0.1

45109 m/p Xylene 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 2 None None None -0.1

45109 m/p Xylene 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 2 None None None -0.1

45109 m/p Xylene 078 102 7 24 HOUR 078 Parts per billion Carbon CARTRIDGE-DNPH-ON-SILICA HPLC ULTRAVIOLET ABSORPTION 0.1 1 None None None -0.1

45109 m/p Xylene 078 108 7 24 HOUR 078 Parts per billion Carbon TEDLAR-BAG-24-HR-SAMPLE GC PHOTOIONIZATION DETECTOR 0.8 3 None None None -0.8

45109 m/p Xylene 078 109 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-SUBAMBIENT-PRESURE GAS CHROMATOGRAPH MASS SELECTIV DET 0.8 2 None None None -0.8

45109 m/p Xylene 078 110 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-PRESSURIZED GAS CHROMATOGRAPH MASS SPECTRO 0.1 1 None None None -0.1

45109 m/p Xylene 078 113 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-PRESSURIZED CAPILLARY GC ITD MASS SPECTRO 0.02 2 None None None -0.02

45109 m/p Xylene 078 116 7 24 HOUR 078 Parts per billion Carbon MIXED SORBENT CARTRIDGE GC/MS 0.32 3 None None None -0.32

45109 m/p Xylene 078 117 7 24 HOUR 078 Parts per billion Carbon TENAX SORBENT CARTRIDGE GC/MS 3.2 2 None None None -3.2

45109 m/p Xylene 078 118 7 24 HOUR 078 Parts per billion Carbon TENAX SORBENT CARTRIDGE GC-FID/ECD 0.08 3 None None None -0.08

45109 m/p Xylene 078 119 7 24 HOUR 078 Parts per billion Carbon PERSONAL PUMP MOLECULAR SIEVE GC/MS 0.08 2 None None None -0.08

45109 m/p Xylene 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

45109 m/p Xylene 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

45109 m/p Xylene 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

45109 m/p Xylene 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

45109 m/p Xylene 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45109 m/p Xylene 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45109 m/p Xylene 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45109 m/p Xylene 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

45109 m/p Xylene 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

45109 m/p Xylene 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

45109 m/p Xylene 078 125 B 3 HOURS 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

45109 m/p Xylene 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.01 2 None None None -0.01

45109 m/p Xylene 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.01 2 None None None -0.01

45109 m/p Xylene 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.01 1 None None None -0.01

45109 m/p Xylene 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.01 1 None None None -0.01

45109 m/p Xylene 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

45109 m/p Xylene 078 129 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER VARIAN SATURN-2 GC/MS 0.01 2 None None None -0.01

45109 m/p Xylene 078 134 J 15 MINUTE 078 Parts per billion Carbon Semi-Continuous Analyzer GC/PID 0.1 1 None None None -0.1

45109 m/p Xylene 078 135 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH CRYFOCUS/VARIAN GC/FINN DTMS 0.1 1 None None None -0.1

45109 m/p Xylene 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

45109 m/p Xylene 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

45109 m/p Xylene 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

45109 m/p Xylene 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 1.34709 4 None None None -1.34709

45109 m/p Xylene 078 144 4 6 HOUR 078 Parts per billion Carbon 3 L SS Canister Subamb press, passive coll GC/Mass Spectro 0.1 2 None None None -0.1

45109 m/p Xylene 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

45109 m/p Xylene 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

45109 m/p Xylene 078 147 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - SATURN II GC/FID 0.68 2 None None None -0.68

45109 m/p Xylene 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

45109 m/p Xylene 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

45109 m/p Xylene 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

45109 m/p Xylene 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

45109 m/p Xylene 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None None -0.1

45109 m/p Xylene 078 151 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER CAPILLARY GC-ECD/PID 0.1 2 None None None -0.1

45109 m/p Xylene 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None None -0.1

45109 m/p Xylene 078 153 7 24 HOUR 078 Parts per billion Carbon Pressurized Canister GC with Multiple Detectors 0.8 2 None None None -0.8

45109 m/p Xylene 078 168 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PACKED COLUMN GC - ECD/PID 4.8 2 None None None -4.8

45109 m/p Xylene 078 169 7 24 HOUR 078 Parts per billion Carbon TEDLAR BAG PACKED COLUMN GC - ECD/PID 4.8 2 None None None -4.8

45109 m/p Xylene 078 171 7 24 HOUR 078 Parts per billion Carbon 6L Pressurized Canister Precon Saturn GC/MS 0.1 2 None None None -0.1

45109 m/p Xylene 078 172 7 24 HOUR 078 Parts per billion Carbon 6L Pressurized Canister Precon HP GC/MS 0.1 2 None None None -0.1

45109 m/p Xylene 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

45109 m/p Xylene 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

45109 m/p Xylene 078 176 6 12 HOUR 078 Parts per billion Carbon 6L SUBATM SS CANISTER ENTECH PRECONCENTRATOR GC/MS 0.4 2 None None None -0.4

45109 m/p Xylene 078 176 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM SS CANISTER ENTECH PRECONCENTRATOR GC/MS 0.4 2 None None None -0.4

45109 m/p Xylene 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

45109 m/p Xylene 078 210 7 24 HOUR 078 Parts per billion Carbon SS 6L Pressurized Canister Cryogenic Precon GC/MS 0.16 3 None None None -0.16

45109 m/p Xylene 078 211 7 24 HOUR 078 Parts per billion Carbon SS Canister Subambient Pressure Gas Chromatograph Mass Spectro 0.54 2 None None None -0.54

43212 n-Butane 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

43212 n-Butane 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43212 n-Butane 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43212 n-Butane 078 104 1 1 HOUR 078 Parts per billion Carbon TENAX/SPHEROCARB-SORBENT-TRAP HEAT DESORPTION GC-FID 0.1 1 None None None -0.1

43212 n-Butane 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43212 n-Butane 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43212 n-Butane 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43212 n-Butane 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43212 n-Butane 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43212 n-Butane 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43212 n-Butane 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43212 n-Butane 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43212 n-Butane 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43212 n-Butane 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43212 n-Butane 078 125 B 3 HOURS 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43212 n-Butane 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43212 n-Butane 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43212 n-Butane 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43212 n-Butane 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43212 n-Butane 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

43212 n-Butane 078 129 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER VARIAN SATURN-2 GC/MS 0.1 1 None None None -0.1

43212 n-Butane 078 135 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH CRYFOCUS/VARIAN GC/FINN DTMS 0.1 1 None None None -0.1

43212 n-Butane 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43212 n-Butane 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43212 n-Butane 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43212 n-Butane 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 0.52688 4 None None None -0.52688

43212 n-Butane 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43212 n-Butane 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43212 n-Butane 078 147 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - SATURN II GC/FID 1.65 2 None None None -1.65

43212 n-Butane 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

43212 n-Butane 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43212 n-Butane 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43212 n-Butane 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43212 n-Butane 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None None -0.1

43212 n-Butane 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None None -0.1

43212 n-Butane 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43212 n-Butane 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43212 n-Butane 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

43238 n-Decane 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

43238 n-Decane 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43238 n-Decane 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43238 n-Decane 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43238 n-Decane 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43238 n-Decane 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43238 n-Decane 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43238 n-Decane 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43238 n-Decane 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43238 n-Decane 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43238 n-Decane 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43238 n-Decane 078 124 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID 1.0 1 None None None -1.0

43238 n-Decane 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.1 1 None None None -0.1

43238 n-Decane 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.1 1 None None None -0.1

43238 n-Decane 078 125 B 3 HOURS 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.1 1 None None None -0.1

43238 n-Decane 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43238 n-Decane 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43238 n-Decane 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43238 n-Decane 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43238 n-Decane 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

43238 n-Decane 078 129 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER VARIAN SATURN-2 GC/MS 0.1 1 None None None -0.1

43238 n-Decane 078 135 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH CRYFOCUS/VARIAN GC/FINN DTMS 0.1 1 None None None -0.1

43238 n-Decane 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43238 n-Decane 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43238 n-Decane 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43238 n-Decane 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 4.27655 4 None None None -4.27655

43238 n-Decane 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43238 n-Decane 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43238 n-Decane 078 147 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - SATURN II GC/FID 0.92 2 None None None -0.92

43238 n-Decane 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

43238 n-Decane 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43238 n-Decane 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43238 n-Decane 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43238 n-Decane 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None None -0.1

43238 n-Decane 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None None -0.1

43238 n-Decane 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43238 n-Decane 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43238 n-Decane 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

43232 n-Heptane 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

43232 n-Heptane 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43232 n-Heptane 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43232 n-Heptane 078 110 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-PRESSURIZED GAS CHROMATOGRAPH MASS SPECTRO 0.1 2 None None None -0.1

43232 n-Heptane 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43232 n-Heptane 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43232 n-Heptane 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43232 n-Heptane 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43232 n-Heptane 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43232 n-Heptane 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43232 n-Heptane 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43232 n-Heptane 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43232 n-Heptane 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43232 n-Heptane 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43232 n-Heptane 078 125 B 3 HOURS 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43232 n-Heptane 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43232 n-Heptane 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43232 n-Heptane 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43232 n-Heptane 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43232 n-Heptane 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

43232 n-Heptane 078 129 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER VARIAN SATURN-2 GC/MS 0.1 1 None None None -0.1

43232 n-Heptane 078 135 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH CRYFOCUS/VARIAN GC/FINN DTMS 0.1 1 None None None -0.1

43232 n-Heptane 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43232 n-Heptane 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43232 n-Heptane 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43232 n-Heptane 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 0.45033 4 None None None -0.45033

43232 n-Heptane 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43232 n-Heptane 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43232 n-Heptane 078 147 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - SATURN II GC/FID 0.93 2 None None None -0.93

43232 n-Heptane 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

43232 n-Heptane 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43232 n-Heptane 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43232 n-Heptane 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43232 n-Heptane 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None None -0.1

43232 n-Heptane 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None None -0.1

43232 n-Heptane 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43232 n-Heptane 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43232 n-Heptane 078 176 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM SS CANISTER ENTECH PRECONCENTRATOR GC/MS 0.08 2 None None None -0.08

43232 n-Heptane 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

43231 n-Hexane 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

43231 n-Hexane 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43231 n-Hexane 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43231 n-Hexane 078 104 1 1 HOUR 078 Parts per billion Carbon TENAX/SPHEROCARB-SORBENT-TRAP HEAT DESORPTION GC-FID 0.1 1 None None None -0.1

43231 n-Hexane 078 110 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-PRESSURIZED GAS CHROMATOGRAPH MASS SPECTRO 0.1 1 None None None -0.1

43231 n-Hexane 078 117 7 24 HOUR 078 Parts per billion Carbon TENAX SORBENT CARTRIDGE GC/MS 0.1 2 None None None -0.1

43231 n-Hexane 078 118 7 24 HOUR 078 Parts per billion Carbon TENAX SORBENT CARTRIDGE GC-FID/ECD 0.01 3 None None None -0.01

43231 n-Hexane 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43231 n-Hexane 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43231 n-Hexane 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43231 n-Hexane 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43231 n-Hexane 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43231 n-Hexane 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43231 n-Hexane 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43231 n-Hexane 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43231 n-Hexane 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43231 n-Hexane 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43231 n-Hexane 078 125 B 3 HOURS 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 1 None None None -0.136

43231 n-Hexane 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43231 n-Hexane 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43231 n-Hexane 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43231 n-Hexane 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43231 n-Hexane 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

43231 n-Hexane 078 129 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER VARIAN SATURN-2 GC/MS 0.1 1 None None None -0.1

43231 n-Hexane 078 135 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH CRYFOCUS/VARIAN GC/FINN DTMS 0.1 1 None None None -0.1

43231 n-Hexane 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43231 n-Hexane 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43231 n-Hexane 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43231 n-Hexane 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 0.29283 4 None None None -0.29283

43231 n-Hexane 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43231 n-Hexane 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43231 n-Hexane 078 147 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - SATURN II GC/FID 0.12 2 None None None -0.12

43231 n-Hexane 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

43231 n-Hexane 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43231 n-Hexane 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43231 n-Hexane 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43231 n-Hexane 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None None -0.1

43231 n-Hexane 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None None -0.1

43231 n-Hexane 078 172 7 24 HOUR 078 Parts per billion Carbon 6L Pressurized Canister Precon HP GC/MS 0.1 2 None None None -0.1

43231 n-Hexane 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43231 n-Hexane 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43231 n-Hexane 078 176 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM SS CANISTER ENTECH PRECONCENTRATOR GC/MS 0.24 2 None None None -0.24

43231 n-Hexane 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

43231 n-Hexane 078 210 7 24 HOUR 078 Parts per billion Carbon SS 6L Pressurized Canister Cryogenic Precon GC/MS 0.04 3 None None None -0.04

43235 n-Nonane 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

43235 n-Nonane 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43235 n-Nonane 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 1 None None None -0.1

43235 n-Nonane 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43235 n-Nonane 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43235 n-Nonane 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43235 n-Nonane 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43235 n-Nonane 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43235 n-Nonane 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43235 n-Nonane 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43235 n-Nonane 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43235 n-Nonane 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 3 None None None -0.136

43235 n-Nonane 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 3 None None None -0.136

43235 n-Nonane 078 125 B 3 HOURS 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 3 None None None -0.136

43235 n-Nonane 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43235 n-Nonane 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43235 n-Nonane 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43235 n-Nonane 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43235 n-Nonane 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

43235 n-Nonane 078 129 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER VARIAN SATURN-2 GC/MS 0.1 1 None None None -0.1

43235 n-Nonane 078 135 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH CRYFOCUS/VARIAN GC/FINN DTMS 0.1 1 None None None -0.1

43235 n-Nonane 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43235 n-Nonane 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43235 n-Nonane 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43235 n-Nonane 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 2.26451 4 None None None -2.26451

43235 n-Nonane 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43235 n-Nonane 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43235 n-Nonane 078 147 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - SATURN II GC/FID 0.94 2 None None None -0.94

43235 n-Nonane 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

43235 n-Nonane 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43235 n-Nonane 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43235 n-Nonane 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43235 n-Nonane 078 150 7 24 HOUR 078 Parts per billion Carbon SS 6L- PRESSURIZED CANISTER CRYOGENIC PRECON: GC/MS 0.1 1 None None None -0.1

43235 n-Nonane 078 152 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-AMBIENT PRECONCENTRATOR GC/FID 0.1 1 None None None -0.1

43235 n-Nonane 078 175 1 1 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43235 n-Nonane 078 175 7 24 HOUR 078 Parts per billion Carbon Passivated Canister Cryogenic Preconcentration GC/MS 0.1 2 None None None -0.1

43235 n-Nonane 078 177 B 3 HOURS 078 Parts per billion Carbon SS Canister Pressurized Preconcentrator GC/FID/MSD 0.1 1 None None None -0.1

43233 n-Octane 078 091 3 4 HOUR 078 Parts per billion Carbon MANUAL FLAME IONIZATION 0.1 1 None None None -0.1

43233 n-Octane 078 101 6 12 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 2 None None None -0.1

43233 n-Octane 078 101 7 24 HOUR 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 2 None None None -0.1

43233 n-Octane 078 101 B 3 HOURS 078 Parts per billion Carbon CANISTER SUBAMBIENT PRESSURE MULTI DETECTOR GC 0.1 2 None None None -0.1

43233 n-Octane 078 110 7 24 HOUR 078 Parts per billion Carbon SS-CANISTER-PRESSURIZED GAS CHROMATOGRAPH MASS SPECTRO 0.1 2 None None None -0.1

43233 n-Octane 078 120 1 1 HOUR 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43233 n-Octane 078 120 B 3 HOURS 078 Parts per billion Carbon SORBANT TUBE-CARBOSIEVE-C-TRAP GAS CHROMATOGRAPH W/FLAME; GC FID 0.1 1 None None None -0.1

43233 n-Octane 078 122 7 24 HOUR 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43233 n-Octane 078 122 B 3 HOURS 078 Parts per billion Carbon 6L AMBIENT CANISTER DUAL FID - PAMS 0.1 1 None None None -0.1

43233 n-Octane 078 123 1 1 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43233 n-Octane 078 123 3 4 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43233 n-Octane 078 123 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43233 n-Octane 078 123 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER DUAL FID - PAMS 0.01 1 None None None -0.01

43233 n-Octane 078 125 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 3 None None None -0.136

43233 n-Octane 078 125 7 24 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 3 None None None -0.136

43233 n-Octane 078 125 B 3 HOURS 078 Parts per billion Carbon PRECONCENTRATION TRAP CHROMPACK AUTOMATED GC- SUBAMB FID 0.136 3 None None None -0.136

43233 n-Octane 078 126 7 24 HOUR 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43233 n-Octane 078 126 B 3 HOURS 078 Parts per billion Carbon SS CANISTER PRESSURIZED CRYOGENIC PRECONCENTRATION GC/FID 0.1 2 None None None -0.1

43233 n-Octane 078 127 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43233 n-Octane 078 127 B 3 HOURS 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER INCOS 50XL GC/MS 0.1 1 None None None -0.1

43233 n-Octane 078 128 1 1 HOUR 078 Parts per billion Carbon PRECONCENTRATION TRAP PE 8700;AUTO GC;SUBAMBIENT-DUAL FID 0.01 2 None None None -0.01

43233 n-Octane 078 129 7 24 HOUR 078 Parts per billion Carbon 6L SUBAMBIENT SS-CANISTER VARIAN SATURN-2 GC/MS 0.1 1 None None None -0.1

43233 n-Octane 078 135 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH CRYFOCUS/VARIAN GC/FINN DTMS 0.1 1 None None None -0.1

43233 n-Octane 078 136 6 12 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43233 n-Octane 078 136 7 24 HOUR 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43233 n-Octane 078 136 B 3 HOURS 078 Parts per billion Carbon INSTRUMENTAL ENTECH 2000 W/ MS/FID 0.1 1 None None None -0.1

43233 n-Octane 078 142 1 1 HOUR 078 Parts per billion Carbon Preconcen trap/Thermal Desorber Auto GC (PE Clarus 500 dual col) 0.69788 4 None None None -0.69788

43233 n-Octane 078 146 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43233 n-Octane 078 146 B 3 HOURS 078 Parts per billion Carbon 6L PRESSURIZED CANISTER PE8700;AUTO GC;SUBAMBIENT-DUAL FID 0.1 1 None None None -0.1

43233 n-Octane 078 147 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - SATURN II GC/FID 0.8 2 None None None -0.8

43233 n-Octane 078 148 7 24 HOUR 078 Parts per billion Carbon 6L PRESSURIZED CANISTER ENTECH PRECON - HP GC/FTIR/MS 0.1 1 None None None -0.1

43233 n-Octane 078 149 1 1 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43233 n-Octane 078 149 7 24 HOUR 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1

43233 n-Octane 078 149 B 3 HOURS 078 Parts per billion Carbon 6L SUBATM CANISTER Entech Precon- GC/FID/MSD 0.1 1 None None None -0.1