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Emission Measurement Center

CFR Promulgated Test Methods (TM)

CFR promulgated test methods have been published in the Federal Register as final rules. These are the official, legal Federal Register Versions.

From the listing below, find the file you would like to download. The available file formats are represented by icons on the right side of the listing. Click on the icon that represents the file format you wish to receive. For an explanation of file formats and their icons, see our TTNWeb File Types.


File Description

Posting Date

File Types

Technical Amendments to Performance Specification 18 and Procedure 6 are on the Proposed Performance Specifications page
Chronology of Methods
Revisions to Test Methods and Testing Regulations; Final Rule, 02/17/2014 03/2015
10/2000 Federal Register Copy of the Amendments for Testing and Monitoring Provisions Exit EPA disclaimer http://www.access.gpo.gov/su_docs/fedreg/a001017c.html
Response to Comments on "Amendments for Testing and Monitoring Provisions" Published in the FR 8/27/97. 02/2001
Preamble to the Amendments for Testing and Monitoring Provisions. 4/2000
Method 1 - Traverse Points - Method FAQs and documents 9/2014
Method 1A - Small Ducts - Method FAQs and documents 8/2013
Method 2 - Velocity - S-type Pitot - Method FAQs and documents 9/2014
Method 2A - Volume Meters - Method FAQs and documents 9/2014
Methos 2B - Exhaust Volume Flow Rate - Method FAQs and documents 9/2014
Method 2C - Standard Pitot - Method FAQs and documents 12/2013
Method 2D - Rate Meters - Method FAQs and documents 9/2014
Method 2E - Landfill Gas Production Flow Rate - Method FAQs and documents 1/2014
Method 2F - Flow Rate Measurement with 3-D Probe - Method FAQs and documents 1/2014
Method 2G - Flow Rate Measurement with 2-D Probe - Method FAQs and documents 1/2014
Method 2H - Flow Rate Measurement with Velocity Decay Near Stack Walls - Method FAQs and documents 1/2014
Memo - New Test Procedures of Stack Gas Flow Rate in Place of Method 2 4/4/2000
Method 3 - Molecular Weight - Method FAQs and documents 9/2014
Method 3A - CO2, O2 - Instrumental - Method FAQs and documents 9/2014
Method 3B - CO2, O2 - Orsat - Method FAQs and documents 1/2015
Method 3C - CO2, CH4, N2, O2 - TCD - Method FAQs and documents 9/2014
Method 4 - Moisture Content - Method FAQs and documents 9/2014
Method 5 - Particulate Matter(PM) - Method FAQs and documents 9/2014
Method 5A - PM Asphalt Roofing - Method FAQs and documents 9/2014
Method 5B - PM Nonsulfuric Acid - Method FAQs and documents 9/2014
Method 5D - PM Baghouses (Particulate Matter) - Method FAQs and documents 9/2014
Method 5E - PM Fiberglass Plants (Particulate Matter) - Method FAQs and documents 9/2014
Method 5F - PM Fluid Catalytic Cracking Unit - Method FAQs and documents 9/2014
Method 5G - PM Wood Heaters from a Dilution Tunnel - Method FAQs and documents 9/2014
Method 5H - PM Wood Heaters from a Stack - Method FAQs and documents 9/2014
Method 5I - Determination of Low Level Particulate Matter Emissions - Method FAQs and documents 9/2014
Method 6 - Sulfur Dioxide (SO2) - Method FAQs and documents 9/2014
Method 6A - SO2, CO2 - Method FAQs and documents 9/2014
Method 6B - SO2, CO2 - Long Term Integrated - Method FAQs and documents 9/2014
Method 6C - SO2 - Instrumental - Method FAQs and documents 9/2014
Method 7 - Nitrogen Oxide (NOx) - Method FAQs and documents 9/2014
Method 7A - NOx - Ion Chromatographic Method - Method FAQs and documents 9/2014
Method 7B - NOx - Ultraviolet Spectrophotometry - Method FAQs and documents 9/2014
Method 7C - NOx - Colorimetric Method - Method FAQs and documents 9/2014
Method 7D - NOx - Ion Chromatographic - Method FAQs and documents 9/2014
Method 7E - NOx - Instrumental - Method FAQs and documents 12/2014
Method 8 - Sulfuric Acid Mist - Method FAQs and documents 9/2014
Method 9 - Visual Opacity - Method FAQs and documents 9/2014
Method 10 - Carbon Monoxide (NDIR) - Method FAQs and documents 9/2014
Method 10A - CO for Certifying CEMS - Method FAQs and documents 9/2014
Method 10B - CO from Stationary Sources - Method FAQs and documents 9/2014
Method 11 - H2S Content of Fuel - Method FAQs and documents 9/2014
Method 12 - Inorganic Lead - Method FAQs and documents 9/2014
Method 13A - Total Fluoride (SPADNS Zirconium Lake) - Method FAQs and documents 9/2014
Method 13B - Total Fluoride (Specific Ion Electrode) - Method FAQs and documents 9/2014
Method 14 - Fluoride for Primary Aluminum Plants - Method FAQs and documents 9/2014
Method 14A - Total Fluoride Emissions from Selected Sources at Primary Aluminum Plants 9/2014
Method 15 - Hydrogen Sulfide, Carbonyl Sulfide, and Carbon Disulfide - Method FAQs and documents 9/2014
Method 15A - Total Reduced Sulfur (TRS Alt.) - Method FAQs and documents 9/2014
Method 16 - Sulfur (Semicontinuous Determination) - Method FAQs and documents 9/2014
Method 16A - Total Reduced Sulfur (Impinger) - Method FAQs and documents 9/2014
Method 16B - Total Reduced Sulfur (GC Analysis) - Method FAQs and documents 9/2014
Method 16C - Total Reduced Sulfur (Real Time Data) - Method FAQs and documents 9/2014
Method 17 - In-Stack Particulate (PM) - Method FAQs and documents 9/2014
Method 18 - VOC by GC - Method FAQs and documents 9/2014
Method 19 - SO2 Removal and PM, SO2, NOx Rates from Electric Utility Steam Generators - Method FAQs and documents 9/2014
Method 20 - NOx from Stationary Gas Turbines - Method FAQs and documents 9/2014
Method 21 - VOC Leaks - Method FAQs and documents 9/2014
Method 22 - Fugitive Opacity - Method FAQs and documents 9/2014
Method 23 - Dioxin and Furan (02/91 FR Copy) - Method FAQs and documents 9/2014
Method 24 - Surface Coatings - Method FAQs and documents 9/2014
Method 24A - Publication Rotogravure Inks and Related Publication Rotogravure Coatings - Method FAQs and documents 9/2014
Method 25 - Gaseous Nonmethane Organic Emissions - Method FAQs and documents 9/2014
Method 25A - Gaseous Organic Concentration (Flame Ionization) - Method FAQs and documents 9/2014
Method 25B - Gaseous Organic Concentration (Infrared Analyzer) - Method FAQs and documents 9/2014
Method 25C - NMOC in Landfill Gases - Method FAQs and documents 9/2014
Method 25D - VOC of Waste Samples - Method FAQs and documents 9/2014
Method 25E- Vapor Phase Organic Concentration in Waste Samples - Method FAQs and documents 9/2014
Method 26 - Hydrogen Chloride, Halides, Halogens - Method FAQs and documents 9/2014
Method 26A - Hydrogen Halide & Halogen-Isokinetic - Method FAQs and documents 9/2014
Method 27 - Vapor Tightness of Gasoline Tank-Pressure Vacuum - Method FAQs and documents 9/2014
Method 28 - Certification and Auditing - Wood Heaters - Method FAQs and documents 9/2014
Method 28A - Air to Fuel Ratio, Burn Rate - Wood-fired Appliances - Method FAQs and documents 9/2014
Method 29 - Metals Emissions from Stationary Sources - Method FAQs and documents 9/2014
Method 30A - Determination of Mercury from Coal-Fired Combustion Sources (Instrumental Analyzer Procedure) - Method FAQs and documents 9/2014
Method 30B - Determination of Mercury from Coal-Fired Combustion Sources Using Carbon Sorbent Traps - Method FAQs and documents 9/2014
Method 101 - Mercury from Chlor-Alkali Plants (Air) - Method FAQs and documents 9/2014
Method 101A - Mercury from Sewage Sludge Incinerators - Method FAQs and documents 9/2014
Method 102 - Mercury from Chlor-Alkali Plants (Hydrogen Streams) - Method FAQs and documents 9/2014
Method 103 - Beryllium Screening Method - Method FAQs and documents 9/2014
Method 104 - Beryllium Emissions Determination - Method FAQs and documents 9/2014
Method 105 -Mercury in Wastewater Treatment Plant Sewage Sludge - Method FAQs and documents 9/2014
Method 106 - Determination of Vinyl Chloride - Method FAQs and documents 9/2014
Method 107 - Vinyl Chloride content of Inprocess Wastewater Samples - Method FAQs and documents 9/2014
Method 107A - Vinyl Choride content of Solvents - Method FAQs and documents 9/2014
Method 108 - Particulate & Gaseous Arsenic emissions - Method FAQs and documents 9/2014
Method 108A - Determination of Arsenic Content in Ore Samples from Nonferrous Smelters - Method FAQs and documents 9/2014
Method 108B - Arsenic - Method FAQs and documents 9/2014
Method 108C - Arsenic - Method FAQs and documents 9/2014
Method 111 - Polonium-210 Emissions - Method FAQs and documents 9/2014
Method 114 - Radionuclide Emissions - Method FAQs and documents 5/1997
Method 115 - Radon-222 Emissions - Method FAQs and documents 4/1996
Method 201 - PM10 - Method FAQs and documents 9/2014
Method 201A - PM10 and PM2.5 (In-stack, CRS) (Revised 12-1-2010) - Method FAQs and documents 12/2014
Method 202 - Condensable Particulate Matter (Revised 12-1-2010) - Method FAQs and documents 9/2014
Methods 203A - Opacity Determination for Time-Averaged Regulations - Method FAQs and documents 8/2013
Methods 203B - Opacity Determination for Time-Exception Regulations - Method FAQs and documents 8/2013
Methods 203C - Opacity Determination for Instantaneous Limitation Regulations - Method FAQs and documents 8/2013
Method 204-204f Preamble. 4/2007
Method 204 - Permanent or Temporary Total Enclosure (TTE) for Determining Capture Efficiency - Method FAQs and documents 9/2014
Method 204A - VOCs in Liquid Input Stream - Method FAQs and documents 9/2014
Method 204B - VOCs in Captured Stream - Method FAQs and documents 9/2014
Method 204C - VOCs in Captured Stream (Dilution Technique) - Method FAQs and documents 9/2014
Method 204D - Fugitive VOCs from Temporary Total Enclosure - Method FAQs and documents 9/2014
Method 204E - Fugitive VOCs from Building Enclosure - Method FAQs and documents 9/2014
Method 204F - VOCs in Liquid Input Stream (Distillation) - Method FAQs and documents 9/2014
Method 205 - Gas Dilution Device Certification Procedure - Method FAQs and documents 9/2014
Method 207 - Presurvey for Corn Wet-Milling Facilities - Method FAQs and documents 3/2012

Method 301 - Method Validation Protocol - Method FAQs and documents

9/2014

Method 303 - By-product Coke Oven Batteries

9/2014
Method 303A - Nonrecovery Coke Oven Batteries - Method FAQs and documents 9/2014
Method 304A - Biodegradation Rates-Vent Option - Method FAQs and documents 12/2014
Method 304B - Biodegradation Rates - Scrubber Option - Method FAQs and documents 12/2014
Method 305 - Potential VOC in Waste - Method FAQs and documents 12/2014
Method 306 - Chromium Emissions Electroplating/Anodizing - Method FAQs and documents 9/2014
Method 306A - Chromium Emissions Electroplating/Anodizing (Mason Jar Method) - Method FAQs and documents 9/2014
Method 306B - Surface Tension for Tanks Electroplating/Anodizing - Method FAQs and documents 12/2014
Method 307 - Emissions from Solvent Vapor Cleaners (Dec. 2, 1994) - Method FAQs and documents 12/2014
Method 308 - Methanol Emissions (Appeared in Federal Register 11/14/97) - Method FAQs and documents 9/2014
Method 310A - Residual Hexane - Method FAQs and documents 3/1997
Method 310B - Residual Solvent - Method FAQs and documents 3/1997
Method 310C - Residual N-Hexane in EDPM Rubber - Method FAQs and documents 3/1997
Method 311 - HAPS in Paints & Coatings - Method FAQs and documents 12/2014
Method 312A - Styrene in SBR Latex (GC) - Method FAQs and documents 3/1997
Method 312B - Styrene in SBR Latex by Capillary GC - Method FAQs and documents 3/1997
Method 312C - Styrene in SBR Latex Produced by Emulsion Polymerization - Method FAQs and documents 3/1997
Method 313A - Residual Hydrocarbon in Rubber Crumb - Method FAQs and documents 3/1997
Method 313B - Residual HC in Rubber Crumb by Capillary GC - Method FAQs and documents 3/1997
Method 315 - PM and MCEM from Aluminum Production Facilities - Method FAQs and documents 9/2014
Method 316 - Sample & Analysis for Formaldehyde emissions in the Mineral Wool & Wool Fiberglass Industries - Method FAQs and documents 9/2014
Method 318 - Extractive FTIR Method for Measurement of Emissions from the Mineral Wool and Wool Fiberglass Industries - Method FAQs and documents 12/2014
Method 320 - Vapor Phase Organic & Inorganic Emissions by Extractive FTIR - Method FAQs and documents 12/2014
Method 321 - Gaseous HCl Emissions at Portland Cement Kilns by FTIR - Method FAQs and documents 9/2014
Method 323 - Formaldehyde Measurement Using Derivitization - Method FAQs and documents 3/2012
Method 325A - Volatile Organic Compounds from Fugitive and Area Sources: Sampler Deployment and VOC Sample Collection - Method FAQs and documents 11/2015
Method 325B - Volatile Organic Compounds from Fugitive and Area Sources: Sampler Preparation and Analysis - Method FAQs and documents 11/2015

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