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Emission Measurement Center Spectral Database

Table 6-7. Compounds Not Meeting Method 301

       Criteria in Hot/Wet Samples


       Carbon Disulfide-028

  SPIKED    DEV.   UNSPIKED   DEV.

   18.39             17.95

   41.90    23.52    36.23    18.28

   58.83             16.59

   63.23     4.41    45.58    28.99

   26.13             41.22

   17.66    -8.47    31.42    -9.80

   61.36              8.14

   45.22   -16.14    38.17    30.03

   19.94             47.29

   54.74    34.81     3.20   -44.09

   40.74    38.12    28.58    23.41


    RSD=    35.71     RSD=    70.99

   Bias=     2.48 Exp Conc=    9.68

      t=     0.10      CF=     0.80

------------------------------------

      Carbon Tetrachloride-029

  SPIKED    DEV.   UNSPIKED   DEV.

    7.33              0.19

    7.37     0.04     0.18    -0.01

    7.42              0.19

    7.43     0.00     0.19     0.00

    7.47              0.25

    7.52     0.05     0.21    -0.05

    7.50              0.21

    7.47    -0.02     0.18    -0.02

    7.59              0.26

    7.54    -0.06     0.20    -0.06

    7.46     0.01     0.21    -0.14


    RSD=     0.37     RSD=    11.87

   Bias=    -2.72 Exp Conc=    9.98

      t=    74.24      CF=     1.37

------------------------------------

         Chloroform-039

  SPIKED    DEV.   UNSPIKED   DEV.

   15.35              0.80

   15.16    -0.19     0.79    -0.01

   15.33              0.69

   15.14    -0.19     0.75     0.06

   15.24              0.91

   15.28     0.05     0.63    -0.28

   15.22              1.03

   15.21    -0.01     0.58    -0.44

   15.60              0.64

   15.51    -0.09     0.78     0.13

   15.49              0.79

   15.20    -0.29     0.63    -0.16

   15.31    -0.72     0.75    -0.70


    RSD=     0.76     RSD=    21.69

   Bias=     4.90 Exp Conc=    9.66

      t=    24.48      CF=     0.66

------------------------------------

           Cumene-046

  SPIKED    DEV.   UNSPIKED   DEV.

   14.68             -0.59

   14.80     0.12    -0.61    -0.02

   14.89             -0.57

   15.07     0.18    -0.60    -0.03

   15.12             -0.59

   15.20     0.09    -0.56     0.03

   15.36             -0.82

   15.58     0.22    -0.54     0.28

   15.69             -0.27

   15.88     0.19    -0.44    -0.16

   15.81             -0.45

   15.91     0.10    -0.44     0.01

   15.33     0.89    -0.54     0.11


    RSD=     0.72     RSD=   -17.61

   Bias=     5.85 Exp Conc=   10.02

      t=    40.11      CF=     0.63

------------------------------------

       1,2-Epoxy Butane-075

  SPIKED    DEV.   UNSPIKED   DEV.

   13.17             -0.41

   13.58     0.41    -0.01     0.40

   14.09             -0.46

   13.81    -0.28    -0.14     0.32

   11.26              1.00

   11.70     0.44     0.26    -0.74

   11.72              0.56

   11.61    -0.10    -0.55    -1.11

    9.79              0.27

   10.76     0.98    -0.19    -0.46

   10.59             -0.49

   10.60     0.01    -0.81    -0.32

   11.89     1.44    -0.08    -1.91


    RSD=     2.87     RSD=  -540.44

   Bias=     1.31 Exp Conc=   10.66

      t=     2.35      CF=     0.89

------------------------------------

        Ethyl Benzene-077

  SPIKED    DEV.   UNSPIKED   DEV.

   14.38             -0.44

   14.45     0.06    -1.02    -0.58

   14.45             -1.11

   14.13    -0.32    -1.14    -0.03

   14.42             -0.68

   14.50     0.08    -1.22    -0.54

   14.41             -1.09

   14.54     0.13    -1.18    -0.10

   14.38             -0.85

   14.42     0.04    -1.20    -0.35

   14.49             -1.27

   14.80     0.31    -1.16     0.11

   14.45     0.30    -1.03    -1.48


    RSD=     0.95     RSD=   -24.58

   Bias=     5.48 Exp Conc=   10.00

      t=    19.02      CF=     0.65

------------------------------------

        Ethylene Oxide-084

  SPIKED    DEV.   UNSPIKED   DEV.

    3.45             -0.44

    2.71    -0.74    -1.16    -0.72

    2.13             -0.93

    2.19     0.07    -0.52     0.41

    3.57             -1.66

    3.35    -0.22    -1.33     0.33

    3.41             -1.90

    3.20    -0.22    -0.70     1.20

    3.52             -1.07

    2.72    -0.80    -1.22    -0.14

    3.34             -0.61

    3.07    -0.27    -0.80    -0.19

    3.06    -2.17    -1.03     0.88


    RSD=    10.99     RSD=   -42.51

   Bias=    -5.92 Exp Conc=   10.00

      t=    10.73      CF=     2.45

------------------------------------

           Methanol-104

 SPIKED    DEV.   UNSPIKED   DEV.

   11.68             -1.19

   12.15     0.47    -1.01     0.19

   12.13             -1.16

   12.30     0.17    -1.17    -0.01

   11.71             -0.92

   11.92     0.21    -1.12    -0.20

   11.80             -1.19

   12.10     0.30    -1.21    -0.02

   11.44             -1.27

   11.90     0.46    -1.18     0.09

   11.81             -1.06

   11.75    -0.07    -1.35    -0.29

   11.89     1.54    -1.15    -0.24


    RSD=     1.88     RSD=   -10.13

   Bias=     4.40 Exp Conc=    8.64

      t=    17.47      CF=     0.66

------------------------------------

       Methyl Bromide-106

  SPIKED    DEV.   UNSPIKED   DEV.

   12.55             -2.66

   13.28     0.73    -3.48    -0.82

   14.45             -3.03

   13.55    -0.89    -2.33     0.70

   14.50             -3.07

   14.54     0.03    -2.59     0.47

   14.32             -2.51

   16.27     1.96    -1.68     0.83

   13.64             -1.79

   12.92    -0.72    -1.65     0.14

   11.76             -3.18

   11.55    -0.21    -3.31    -0.13

   13.61     0.90    -2.61     1.20


    RSD=     5.07     RSD=   -16.11

   Bias=     6.24 Exp Conc=    9.98

      t=     7.72      CF=     0.62

------------------------------------

       Methyl Chloroform-108

  SPIKED    DEV.   UNSPIKED   DEV.

   10.49              4.78

   10.55     0.06     4.42    -0.36

   10.58              4.44

   10.33    -0.26     4.54     0.10

   10.41              4.48

   10.42     0.01     4.55     0.07

   10.46              4.54

   10.40    -0.06     4.54     0.01

   10.33              4.53

   10.35     0.02     4.52    -0.01

   10.22              4.46

   10.27     0.05     4.54     0.09

   10.40    -0.18     4.53    -0.10


    RSD=     0.77     RSD=     2.47

   Bias=    -2.77 Exp Conc=    8.64

      t=    20.10      CF=     1.47

------------------------------------

        Methyl Iodide-111

  SPIKED    DEV.   UNSPIKED   DEV.

    8.02             -1.28

    7.39    -0.63    -0.66     0.62

    6.85             -0.63

    6.62    -0.23     0.00     0.63

    7.83             -0.57

    7.97     0.14    -0.09     0.49

    7.88              0.10

    7.64    -0.24     0.47     0.37

    7.87             -0.50

    7.28    -0.59    -0.43     0.07

    6.91             -0.31

    6.20    -0.72    -0.27     0.04

    7.37    -2.26    -0.35     2.21


    RSD=     4.60     RSD=   -89.10

   Bias=    -2.32 Exp Conc=   10.04

      t=     5.05      CF=     1.30

------------------------------------

     Methyl Isobutyl Ketone-112

  SPIKED    DEV.   UNSPIKED   DEV.

   20.98              4.10

   21.25     0.28     4.46     0.36

   21.31              4.50

   21.05    -0.26     4.42    -0.09

   21.09              4.39

   21.38     0.30     4.45     0.07

   21.21              4.52

   21.18    -0.03     4.56     0.04

   20.93              4.35

   21.22     0.29     4.48     0.13

   21.18              4.60

   21.09    -0.08     4.47    -0.14

   21.16     0.50     4.44     0.37


    RSD=     0.77     RSD=     2.74

   Bias=     6.71 Exp Conc=   10.00

      t=    32.89      CF=     0.60

------------------------------------

     Methyl t-Butyl Ether-115

  SPIKED    DEV.   UNSPIKED   DEV.

   -2.85             -0.68

   -2.60     0.25    -0.38     0.30

   -2.27             -0.60

   -2.08     0.19    -0.39     0.21

   -1.31             -0.60

   -0.52     0.78    -0.37     0.23

    0.04             -0.49

    0.71     0.67    -0.34     0.15

    1.43             -0.67

    2.13     0.70    -0.50     0.17

    2.44             -0.44

    2.61     0.17    -0.43     0.01

   -0.19     2.76    -0.49     1.07


    RSD=  -196.95     RSD=   -28.61

   Bias=    -9.34 Exp Conc=    9.64

      t=    23.41      CF=    31.90

------------------------------------

      Methylene Chloride-117

  SPIKED    DEV.   UNSPIKED   DEV.

    9.60              0.65

   10.42     0.82     1.03     0.38

   10.81             -0.47

   10.94     0.13     0.41     0.88

   10.69              0.60

   10.85     0.16     0.18    -0.42

   10.73              0.08

   11.47     0.74     0.29     0.21

   10.37              0.31

   10.37     0.00     0.16    -0.15

   10.61              0.19

   11.02     0.40    -0.19    -0.37

   10.65     2.26     0.27     0.52


    RSD=     3.23     RSD=   121.81

   Bias=     0.36 Exp Conc=   10.02

      t=     0.77      CF=     0.96

------------------------------------

      Propylene Oxide-143

  SPIKED    DEV.   UNSPIKED   DEV.

   -1.11             -4.17

   -2.90    -1.80    -4.00     0.17

   -2.58             -3.46

   -1.91     0.66    -3.39     0.07

   -1.97             -4.29

   -4.04    -2.06    -3.60     0.69

   -1.86             -3.48

   -3.68    -1.82    -4.17    -0.69

   -2.63             -4.25

   -3.13    -0.50    -3.29     0.96

   -1.98             -3.02

   -3.08    -1.10    -4.42    -1.40

   -2.57    -6.62    -3.79    -0.20


    RSD=   -40.01     RSD=   -14.94

   Bias=    -8.82 Exp Conc=   10.04

      t=     7.50      CF=     8.21

------------------------------------

           Styrene-147

  SPIKED    DEV.   UNSPIKED   DEV.

   14.04              2.87

   13.80    -0.24     1.02    -1.85

   13.84              1.34

   13.92     0.09     1.05    -0.29

   14.10              1.25

   14.40     0.30    -0.43    -1.69

   14.31             -0.12

   14.18    -0.13     0.00     0.12

   13.65              0.60

   13.97     0.32     0.45    -0.15

   14.23              0.67

   14.08    -0.15     0.67     0.00

   14.04     0.18     0.78    -3.86


    RSD=     1.11     RSD=    93.36

   Bias=     2.50 Exp Conc=   10.76

      t=     3.35      CF=     0.81

------------------------------------

     Tetrachloroethylene-151

  SPIKED    DEV.   UNSPIKED   DEV.

   10.45             -0.09

   10.65     0.20    -0.10    -0.01

   10.60             -0.10

   10.70     0.10    -1.17    -1.07

   10.53             -0.01

   10.63     0.10    -0.08    -0.07

   10.68             -0.10

   10.60    -0.08    -0.09     0.02

   10.56             -0.06

   10.57     0.01    -0.06     0.00

   10.62             -0.11

   10.62    -0.01    -0.11     0.00

   10.60     0.32    -0.17    -1.14


    RSD=     0.70     RSD=  -179.94

   Bias=     0.77 Exp Conc=   10.00

      t=     2.43      CF=     0.93

------------------------------------

           Toluene-153

  SPIKED    DEV.   UNSPIKED   DEV.

   14.13              0.94

   14.41     0.29     0.51    -0.43

   14.39              0.23

   14.31    -0.08     0.31     0.08

   14.45              0.32

   14.54     0.10     0.34     0.03

   14.59              0.69

   14.22    -0.37     0.13    -0.55

   13.94              0.13

   13.73    -0.21     0.35     0.22

   14.02              0.07

   13.86    -0.16     0.03    -0.04

   14.22    -0.44     0.34    -0.70


    RSD=     1.12     RSD=    63.78

   Bias=     4.12 Exp Conc=    9.76

      t=    15.42      CF=     0.70

------------------------------------

          o-Xylene-171

  SPIKED    DEV.   UNSPIKED   DEV.

   14.17             -3.36

   14.16    -0.01    -3.11     0.25

   14.06             -3.22

   14.31     0.24    -3.32    -0.10

   14.09             -2.93

   14.14     0.05    -3.04    -0.11

   14.22             -3.18

   14.12    -0.10    -3.02     0.15

   14.11             -2.96

   14.43     0.33    -3.04    -0.09

   14.32             -2.90

   14.43     0.11    -3.13    -0.23

   14.21     0.62    -3.10    -0.12


    RSD=     0.88     RSD=    -3.76

   Bias=     7.31 Exp Conc=   10.00

      t=    42.66      CF=     0.58

------------------------------------

           m-Xylene-172

  SPIKED    DEV.   UNSPIKED   DEV.

   14.02             -2.68

   14.28     0.27    -2.49     0.19

   14.34             -2.55

   14.60     0.27    -2.66    -0.10

   14.11             -2.69

   14.63     0.53    -2.74    -0.05

   14.45             -2.87

   14.46     0.02    -2.75     0.12

   14.42             -2.46

   14.20    -0.21    -2.39     0.07

   14.35     0.86    -2.63     0.23


    RSD=     1.50     RSD=    -3.17

   Bias=     6.98 Exp Conc=   10.00

      t=    30.29      CF=     0.59

------------------------------------

           Acetone-192

  SPIKED    DEV.   UNSPIKED   DEV.

   -0.21            -11.40

    0.00     0.21   -11.59    -0.19

   -0.13            -11.70

    0.08     0.21   -11.77    -0.07

   -0.32            -11.94

   -0.10     0.22   -11.89     0.05

   -0.10            -11.67

    0.01     0.11   -11.71    -0.04

   -0.16            -11.67

    0.16     0.31   -11.59     0.08

    0.04            -11.85         
	   

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