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Emission Measurement Center Spectral Database

Table 6.3 Compounds Meeting Method 301 Criteria in Hot/Wet Samples

                  Acetonitrile-003

           SPIKED     DEV.   UNSPIKED   DEV.

            12.59              3.35

            14.56     1.96     4.19     0.85

            16.77              3.70

            14.86    -1.91     3.12    -0.58

            16.45              3.39

            16.58     0.13     5.81     2.42

            15.00              4.55

            15.84     0.85     4.02    -0.53

            14.97              3.48

            17.76     2.79     3.31    -0.16

            16.13              3.69

            13.49    -2.65     5.43     1.75

            15.42     1.17     4.00     3.74


             RSD=     8.99     RSD=    23.10

            Bias=     0.91 Exp Conc=   10.50

               t=     0.55      CF=     0.92

         ------------------------------------

                   Acrolein-006

           SPIKED     DEV.   UNSPIKED   DEV.

            11.06             -1.15

            11.04    -0.02    -1.35    -0.20

            11.24             -1.36

            11.36     0.12    -1.24     0.12

            11.08             -1.24

            11.33     0.25    -1.02     0.23

            11.21             -1.14

            11.26     0.05    -1.11     0.03

            11.17             -1.12

            11.01    -0.16    -1.11     0.01

            11.23             -0.86

            11.21    -0.02    -1.13    -0.27

            11.18     0.23    -1.15    -0.09


             RSD=     0.84     RSD=   -10.69

            Bias=     0.75 Exp Conc=   11.58

               t=     4.86      CF=     0.94

         ------------------------------------

                 Acrylonitrile-009

           SPIKED     DEV.   UNSPIKED   DEV.

            12.08              1.64

            12.25     0.17     1.71     0.07

            12.15              1.79

            12.27     0.12     1.70    -0.09

            11.98              1.79

            12.10     0.12     1.85     0.06

            12.15              1.74

            12.38     0.23     1.88     0.14

            12.04              1.79

            12.28     0.24     1.75    -0.04

            12.30              1.60

            12.36     0.06     1.72     0.12

            12.19     0.93     1.75     0.27


             RSD=     0.97     RSD=     3.82

            Bias=     0.45 Exp Conc=   10.00

               t=     3.28      CF=     0.96

         ------------------------------------

                 Allyl Chloride-010

           SPIKED     DEV.   UNSPIKED   DEV.

             6.23             -4.50

             6.36     0.13    -5.52    -1.02

             6.12             -5.22

             6.40     0.28    -5.39    -0.17

             6.00             -5.18

             6.40     0.40    -5.12     0.06

             6.41             -5.44

             6.26    -0.15    -5.33     0.11

             5.87             -5.52

             6.27     0.40    -6.00    -0.49

             6.01             -5.95

             6.43     0.42    -5.85     0.09

             6.23     1.48    -5.42    -1.42


             RSD=     3.62     RSD=    -6.13

            Bias=     1.45 Exp Conc=   10.20

               t=     3.60      CF=     0.88

         ------------------------------------

                     Benzene-015

           SPIKED     DEV.   UNSPIKED   DEV.

            10.64             -0.57

            10.89     0.25    -0.45     0.12

            10.93             -0.51

            11.10     0.17    -0.45     0.06

            10.69             -0.16

            11.02     0.33    -0.23    -0.07

            11.12             -0.14

            11.17     0.05    -0.28    -0.14

            10.84             -0.15

            11.06     0.22    -0.23    -0.08

            11.12             -0.21

            10.98    -0.14    -0.24    -0.03

            10.96     0.88    -0.30    -0.14


             RSD=     1.38     RSD=   -21.20

            Bias=     1.27 Exp Conc=   10.00

               t=     7.72      CF=     0.89

         ------------------------------------

                   Bromoform-022

           SPIKED     DEV.   UNSPIKED   DEV.

             9.69             -0.51

             9.79     0.09    -0.48     0.03

             9.85             -0.53

             9.91     0.06    -0.60    -0.08

             9.85             -0.42

            10.09     0.24    -0.42     0.00

            10.08             -0.41

            10.07    -0.01    -0.39     0.02

            10.20             -0.31

            10.04    -0.16    -0.44    -0.13

             9.96     0.22    -0.45    -0.16


             RSD=     0.98     RSD=   -10.91

            Bias=     0.55 Exp Conc=    9.86

               t=     5.00      CF=     0.95

         ------------------------------------

                  1,3-Butadiene-023

           SPIKED     DEV.   UNSPIKED   DEV.

             7.02             -2.25

             7.12     0.11    -2.36    -0.11

             7.10             -2.54

             6.97    -0.13    -2.39     0.15

             6.93             -2.45

             6.85    -0.08    -1.76     0.69

             6.92             -2.03

             7.03     0.11    -2.11    -0.08

             6.46             -2.30

             6.73     0.27    -2.36    -0.06

             6.80             -2.54

             6.82     0.02    -2.58    -0.04

             6.90     0.30    -2.31     0.55


             RSD=     1.44     RSD=    -9.09

            Bias=    -0.52 Exp Conc=    9.72

               t=     2.23      CF=     1.06

         ------------------------------------

               Carbonyl Sulfide-030

           SPIKED     DEV.   UNSPIKED   DEV.

            10.53              0.13

            10.53     0.01     0.09    -0.04

            10.58              0.08

            10.69     0.11     0.12     0.05

            10.56              0.15

            10.65     0.09     0.15     0.00

            10.61              0.14

            10.59    -0.02     0.11    -0.02

            10.43              0.21

            10.44     0.01     0.18    -0.03

            10.47              0.09

            10.43    -0.04     0.09     0.00

            10.54     0.16     0.13    -0.05


             RSD=     0.41     RSD=    16.02

            Bias=    -0.29 Exp Conc=   10.70

               t=     5.96      CF=     1.03

         ------------------------------------

                 Chlorobenzene-037

           SPIKED     DEV.   UNSPIKED   DEV.

             9.52             -3.16

             9.41    -0.11    -3.23    -0.07

             9.83             -3.44

            10.00     0.16    -3.12     0.32

             9.58             -3.00

             9.56    -0.02    -2.79     0.22

             9.61             -3.09

             9.55    -0.06    -3.03     0.06

             9.99             -3.23

             9.87    -0.13    -3.11     0.12

             9.92             -1.44

             9.89    -0.03    -2.88    -1.44

             9.73    -0.18    -2.96    -0.80


             RSD=     0.72     RSD=   -14.61

            Bias=     2.69 Exp Conc=   10.00

               t=     6.13      CF=     0.79

         ------------------------------------

                Ethyl Chloride-079

           SPIKED     DEV.   UNSPIKED   DEV.

             7.16             -4.19

             7.68     0.52    -3.99     0.20

             7.13             -4.31

             7.75     0.62    -4.34    -0.03

             7.40             -5.41

             8.52     1.12    -5.26     0.15

             7.11             -5.15

             8.13     1.03    -5.42    -0.27

             6.11             -6.14

             6.64     0.54    -6.09     0.06

             6.12             -6.07

             5.94    -0.19    -6.48    -0.42

             7.14     3.64    -5.24    -0.31


             RSD=     7.33     RSD=    -3.09

            Bias=     1.48 Exp Conc=   10.90

               t=     2.70      CF=     0.88

         ------------------------------------

               Ethylene Dibromide-080

           SPIKED     DEV.   UNSPIKED   DEV.

             8.98             -1.07

             9.11     0.13    -0.93     0.14

             9.14             -0.97

             9.29     0.16    -0.96     0.01

             9.11             -0.83

             9.09    -0.02    -1.01    -0.18

             9.14             -0.98

             9.20     0.06    -0.98    -0.01

             9.17             -0.94

             9.16    -0.01    -1.02    -0.08

             9.31             -1.09

             9.21    -0.11    -1.10    -0.01

             9.16     0.20    -0.99    -0.13


             RSD=     0.75     RSD=    -7.01

            Bias=     1.03 Exp Conc=    9.12

               t=    10.57      CF=     0.90

         ------------------------------------

                   n-Hexane-095

           SPIKED     DEV.   UNSPIKED   DEV.

            10.08             -0.71

            10.42     0.34    -0.75    -0.03

            10.49             -0.81

            10.54     0.05    -0.80     0.01

            10.52             -0.38

            10.61     0.08    -0.57    -0.19

            10.55             -0.62

            10.86     0.31    -0.61     0.01

            10.33             -0.42

            10.48     0.16    -0.55    -0.13

            10.58             -0.60

            10.78     0.19    -0.64    -0.04

            10.52     1.13    -0.62    -0.37


             RSD=     1.46     RSD=   -10.94

            Bias=     1.20 Exp Conc=    9.94

               t=     7.15      CF=     0.89

         ------------------------------------

              Methyl Chloride-107

           SPIKED     DEV.   UNSPIKED   DEV.

             7.81             -1.05

             7.55    -0.26    -1.10    -0.04

             7.75             -2.04

             7.68    -0.06    -1.78     0.26

             7.30             -2.50

             7.29    -0.01    -2.27     0.23

             7.19             -2.03

             8.12     0.92    -2.32    -0.29

             7.56             -2.51

             7.72     0.17    -2.39     0.12

             7.65             -2.40

             7.70     0.05    -2.29     0.11

             7.61     0.81    -2.06     0.38


             RSD=     3.71     RSD=    -6.79

            Bias=    -0.33 Exp Conc=   10.00

               t=     1.06      CF=     1.03

         ------------------------------------

              Methyl Ethyl Ketone-109

           SPIKED     DEV.   UNSPIKED   DEV.

             6.59             -3.88

             5.83    -0.76    -5.26    -1.39

             7.01             -5.93

             6.37    -0.64    -5.48     0.45

             6.26             -6.67

             6.25    -0.02    -6.43     0.24

             6.43             -6.16

             6.34    -0.09    -6.42    -0.26

             6.96             -6.11

             6.24    -0.72    -6.11     0.00

             6.75             -5.75

             6.93     0.18    -5.74     0.01

             6.50    -2.05    -5.83    -0.95


             RSD=     5.52     RSD=    -7.42

            Bias=     3.36 Exp Conc=    8.96

               t=     5.99      CF=     0.73

         ------------------------------------

             Methyl Methacrylate-114

           SPIKED     DEV.   UNSPIKED   DEV.

             8.38             -2.42

             8.39     0.01    -2.53    -0.11

             8.61             -2.62

             8.63     0.02    -2.55     0.07

             8.17             -2.34

             8.32     0.16    -2.48    -0.14

             8.42             -2.55

             8.63     0.21    -2.50     0.04

             8.48             -2.15

             8.36    -0.12    -2.34    -0.19

             8.58             -2.31

             8.53    -0.05    -2.38    -0.07

             8.46     0.22    -2.43    -0.39


             RSD=     0.99     RSD=    -3.34

            Bias=     0.79 Exp Conc=   10.10

               t=     6.74      CF=     0.93

         ------------------------------------

               2-Nitropropane-124

           SPIKED     DEV.   UNSPIKED   DEV.

             9.92              0.84

            10.06     0.14     0.28    -0.56

            10.19              0.30

            10.13    -0.07     0.52     0.22

            10.22              0.52

            10.27     0.05     0.69     0.17

            10.25              0.58

            10.24    -0.01     0.50    -0.08

            10.08              0.83

             9.98    -0.10     0.61    -0.22

            10.08              0.58

            10.04    -0.04     0.60     0.02

            10.12    -0.03     0.57    -0.45


             RSD=     0.56     RSD=    33.69

            Bias=     0.57 Exp Conc=    8.98

               t=     2.84      CF=     0.94

         ------------------------------------

             Propylene Dichloride-142

           SPIKED     DEV.   UNSPIKED   DEV.

            11.83              1.27

            11.90     0.07     1.17    -0.10

            11.64              1.12

            11.70     0.06     1.10    -0.02

            11.10              1.23

            11.28     0.18     0.82    -0.41

            11.20              0.83

            11.06    -0.15     0.89     0.06

            10.58              1.10

            10.78     0.20     0.86    -0.24

            10.99              1.20

            11.02     0.03     0.98    -0.22

            11.26     0.39     1.05    -0.94


             RSD=     0.83     RSD=    14.90

            Bias=    -0.27 Exp Conc=   10.48

               t=     1.48      CF=     1.03

         ------------------------------------

              1,1,2-Trichloroethane-159

           SPIKED     DEV.   UNSPIKED   DEV.

             0.89            -11.34

             0.89     0.00   -11.29     0.05

             0.93            -11.87

             1.05     0.12   -11.45     0.42

             0.78            -11.25

             0.84     0.06   -10.87     0.38

             0.95            -11.17

             0.93    -0.02   -11.19    -0.02

             1.19            -11.32

             1.27     0.08   -11.31     0.01

             1.28             -9.59

             1.38     0.11   -11.30    -1.71

             1.03     0.34   -11.16    -0.87


             RSD=     5.26     RSD=    -4.66

            Bias=     2.19 Exp Conc=   10.00

               t=     4.19      CF=     0.82

         ------------------------------------

                Trichlorothylene-160

           SPIKED     DEV.   UNSPIKED   DEV.

             9.95             -0.40

            10.03     0.08    -0.42    -0.01

            10.02             -0.43

            10.03     0.01    -0.44    -0.01

            10.07             -0.40

            10.22     0.16    -0.56    -0.16

            10.17             -0.56

            10.20     0.03    -0.53     0.03

             9.74             -0.38

             9.97     0.23    -0.49    -0.10

            10.13             -0.47

            10.07    -0.05    -0.45     0.01

            10.05     0.45    -0.46    -0.24


             RSD=     0.85     RSD=   -12.16

            Bias=     1.03 Exp Conc=    9.48

               t=    10.07      CF=     0.90

         ------------------------------------

             2,2,4-Trimethylpentane-165

           SPIKED     DEV.   UNSPIKED   DEV.

            10.60             -0.16

            10.68     0.08    -0.15     0.00

            10.70             -0.16

            10.70     0.00    -0.17    -0.01

            10.65             -0.09

            10.83     0.18    -0.17    -0.08

            10.81             -0.16

            10.78    -0.04    -0.17    -0.01

            10.82             -0.08

            10.74    -0.08    -0.16    -0.07

            10.73     0.15    -0.15    -0.17


             RSD=     0.62     RSD=   -23.74

            Bias=     0.90 Exp Conc=    9.98

               t=    11.92      CF=     0.92

         ------------------------------------

                Vinyl Acetate-166

           SPIKED     DEV.   UNSPIKED   DEV.

             2.41             -7.63

             2.96     0.55    -8.59    -0.96

             2.85             -7.84

             3.94     1.09    -8.02    -0.18

             3.14             -8.11

            -0.04    -3.18    -6.84    -1.27

             4.11             -6.93

             2.45    -1.66    -8.54    -1.61

             2.43             -7.52

             1.38    -1.05    -6.18     1.34

             3.26             -6.01

             1.50    -1.76    -8.38    -2.37

             2.53    -6.02    -7.55    -2.50


             RSD=    49.09     RSD=   -13.56

            Bias=     0.04 Exp Conc=   10.04

               t=     0.03      CF=     1.00

         ------------------------------------

                 Vinyl Bromide-167

           SPIKED     DEV.   UNSPIKED   DEV.

             9.93              0.30

             9.85    -0.07     0.34     0.04

             9.83              0.34

             9.87     0.03     0.36     0.02

             9.91              0.40

            10.01     0.10     0.35    -0.05

            10.06              0.34

             9.98    -0.07     0.38     0.04

            10.07              0.33

            10.09     0.02     0.45     0.12

            10.23              0.32

            10.00    -0.23     0.44     0.12

             9.99    -0.22     0.36     0.28


             RSD=     0.79     RSD=    15.00

            Bias=    -0.38 Exp Conc=   10.00

               t=     3.90      CF=     1.04

         ------------------------------------

                 Vinyl Chloride-168

           SPIKED     DEV.   UNSPIKED   DEV.

            11.22             -1.89

            11.16    -0.06    -1.88     0.02

            11.34             -1.88

            11.27    -0.08    -1.96    -0.08

            11.07             -1.94

            11.17     0.10    -1.96    -0.02

            11.13             -1.86

            11.10    -0.03    -1.95    -0.10

            11.21             -2.15

            11.00    -0.21    -2.06     0.09

            11.03             -1.27

            10.99    -0.03    -1.54    -0.27

            11.14    -0.32    -1.86    -0.35


             RSD=     0.66     RSD=    -4.74

            Bias=     3.00 Exp Conc=   10.00

               t=    26.11      CF=     0.77

         ------------------------------------

              Vinylidene Chloride-169

           SPIKED     DEV.   UNSPIKED   DEV.

            10.32              0.33

            10.32     0.00     0.41     0.08

            10.30              0.34

            10.32     0.02     0.33    -0.01

            10.49              0.40

            10.43    -0.06     0.36    -0.04

            10.42              0.46

            10.43     0.01     0.35    -0.11

            10.18              0.40

            10.07    -0.11     0.35    -0.05

            10.11              0.31

            10.10    -0.01     0.27    -0.04

            10.29    -0.17     0.36    -0.17


             RSD=     0.37     RSD=    12.29

 

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